Experimental data on biotite-melt trace-element partitioning

Creator(s):
Beard, Charles D; ORCID: 0000-0001-6221-6868
van Hinsberg, Vincent J
Stix, John
Humphreys, Madeleine CS
Weller, Owen M
Abstract:
Biotite is a key hydrous silicate mineral in evolved magmatic systems, but its control on the behaviour of minor- and trace-elements, in particular the REE, Nb, Li, and F is not well understood. Here, we quantify that control in sodic (per)alkaline H2O-saturated magmas with variable F-content through crystallisation experiments at 650--800ºC and 200 MPa total pressure, at log fO2 ~FMQ +1. Biotite-glass pairs from tephriphonolite to phonolite fall deposits from Tenerife, Canary Islands, complement our experimental data set. The biotite-melt Kd F/OH exchange coefficients are 2.9–47.0, typically 6.5–12.5, with minima for Al-rich, Mg-poor biotite. Lithium partition coefficients are 0.24–32.8 with minima in Si-poor biotite formed at high temperatures. D values for the large alkali metal ions Na–Cs define Onuma parabole consistent with their incorporation on the biotite XII A-site. Niobium partition coefficients are 0.1–1.2, and highest in Ti-rich biotite. The REE and actinides have D values less than 0.01 as their ionic radii fall between the size of the XII A-site and VI M-sites of biotite. Our data, alongside a literature compilation constrain empirical models that: (1) describe the exchange of F and OH between the silicate melt and the biotite W-site; (2) predict the partitioning of 1+ cations Li–Cs between silicate melt and the biotite A- and M-sites; (3) predict D Nb values. The models use the major-element composition of biotite and melt, pressure and temperature as input. Models are calibrated for use over a wide range of $P$-$T$-$X$ and can be used to interrogate biotite from natural systems to determine the composition of their source melt, or to forward model the trace-element evolution of mafic to evolved igneous systems at upper-mantle to crustal pressures.
How to cite this dataset:
Beard, C. D., van Hinsberg, V. J., Stix, J., Humphreys, M. C., Weller, O. M., 2025. Experimental data on biotite-melt trace-element partitioning, Version 1.0. Interdisciplinary Earth Data Alliance (IEDA). https://doi.org/10.60520/IEDA/113921. Accessed 2025-08-14.
DOI Creation Date:
2025-08-08
Publication DOI:
License:
Creative Commons Attribution 4.0 International [CC-BY-4.0]
Funding source(s):
Geotop Centre de recherche sur la dynamique du système Terre
DIVEX: Diversification de l''Exploration Minérale au Québec
Society of Economic Geologists Canada Foundation
UK Research and Innovation Natural Environment Research Council
Natural Sciences and Engineering Research Council of Canada
User Contributed Keyword(s):
Experimental petrology; Halogens; Mica group; Partition coefficient; Pegmatite
Data Available On:
2025-08-09
Resource Type:
Dataset
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